Tuesday 05/28/13

10:10 A – 5:30 P

RNA labeling of cultured cells

  • incubate cells in 55C RNA hybe buffer, 30 min
  • transfer to RT 2x SSC, wash 10 min
  • transfer to PBT wash 10 min+ 2x
  • block 1 hour
  • stain with shp anti-dig, 1 hr
  • rinse
  • block
  • stain with 555 anti-shp

Cell culture

  • Dilute cells 1:3 in new media, passage cells into new flask
  • Move to 28C to grow until Thursday.

Probe making

  • test gel.
  • lanes not at all as expected
  • new test PCR: Try different library concentrations and primer concentrations.
    • library 2x (1 uL in 50)
    • library 2/5x (dilute 1:5, then add 1 in 50 uL)
    • library 1x + primer 0.2x
    • library 1x + primers 2x
    • Gel order: 3R, BXC, Ubx-a, AbdA-a, AbdB-a
  • gel extract lower T7 bands (gel was taken by another?)
    primer_libconc_effect

STORM

  • finish imaging y-locus
  • start imaging black locus. Spots much more visible and much longer lived when viewed in imaging buffer with Glox. (should try this with my new POSS).
  • STORM switching of k locus pretty good, recording 85K frames.
  • setup run. Recorded 3 positions, then aborted to test pyranose.

Imaging

  • Make fresh make pyranose oxidase for pH stable switching: 6 mg in 100uL im buffer + 100uL catalase for 100x stock. Labeled as P.O.S.S. (Pyranose Oxygen Scavenging System)
  • test POSS vs glucose on DNA. 1x POS = substantially less switching than 1x GLOX. 1/10 x POS is even worse. 10x POS is comparible. 10x Similar mass ratio to glucose oxidase, which I normally do at 18 mg per 100 uL.
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